Journal Article

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Acta crystallographica.Section E, Crystallographic communications

Acta Crystallogr.E.Crystallogr.Commun.

17-Jan

71

Pt 2

176

179

LR: 20150418; JID: 101648987; OID: NLM: PMC4384575; OTO: NOTNLM; 2015/02/01 [ecollection]; 2014/12/31 [received]; 2015/01/06 [accepted]; 2015/01/17 [epublish]; epublish

England

2056-9890

PMID: 25878812

eng

Journal Article

10.1107/S2056989015000195 [doi]

Unknown(0)

25878812

In the cyclo-hexene ring of the title compound, C23H20BrNO3S, the -(CH2)4- atoms are positionally disordered [occupancy ratio = 0.753 (6):0.247 (6)]. The ring has a half-chair conformation for both the major and minor components. The dihedral angles between the mean plane of the thio-phene ring and those of the benzene and phenyl rings are 35.2 (4) and 57.7 (3) degrees , respectively. The planes of the two aryl rings are twisted with respect to each other by 86.4 (6) degrees . In the mol-ecule, there is an O-Hcdots, three dots, centeredN hydrogen bond forming an S(6) ring motif. In the crystal, mol-ecules are linked via C-Hcdots, three dots, centeredO hydrogen bonds, forming chains parallel to [100].

Kaur,M., Jasinski,J.P., Yathirajan,H.S., Glidewell,C., Byrappa,K.

Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India.; Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USA.; Department of Studies in Chemistry, University of Mysore, Manasaga

20150117

PMC4384575

http://vp9py7xf3h.search.serialssolutions.com/?charset=utf-8&pmid=25878812

2015